Pengaruh Variasi Waktu Peleburan Terhadap Konduktivitas Listrik Zeolit dari Abu Dasar Batubara yang Disintesis dengan Metode Peleburan Alkali Hidrotermal

Authors

  • Nurhabibah Nurhabibah Jurusan Fisika FMIPA Universitas Andalas
  • Afdhal Muttaqin Jurusan Fisika FMIPA Universitas Andalas

DOI:

https://doi.org/10.25077/jfu.6.3.240-246.2017

Abstract

Telah dilakukan sintesis zeolit dari abu dasar batubara menggunakan metode peleburan alkali hidrotermal dengan variasi waktu peleburan.Variasi waktu peleburan yang digunakan adalah 1 jam (Z1), 2 jam (Z2), 3 jam (Z2), dan 4 jam (Z4). Abu dasar dan NaOH dilebur dengan perbandingan 1:1,2. Sampel yang telah dilebur, kemudiandipanaskanmelalui proses hidrotermal dengan medium kristalisasi NaAlO2. Sampel zeolit kemudian dinetralkan dengan aquades hingga mencapai pH 9-10. Sampel dikarakterisasi menggunakan XRD dengan software Match! 3. Konduktivitas listrik sampel diukur dengan LCR-meter. Hasil XRD menunjukkan bahwa sampel Z1 mengandung sodalit, lazurit, katoit, megakalsilit serta masih terdapat kuarsa dan kristobalit. Sampel Z2 mengandung sodalit, leusit dan kalsilit. Sampel Z3 mengandung sodalit dan bohmit, serta sampel Z4 mengandung sodalit, nosean dan katoit. Konduktivitas listrik yang dihasilkan berkisar dari 0,8 × 10-6 – 2,4 × 10-6 S/cm dan berada pada rentang bahan semikonduktor. Zeolit dengan waktu peleburan selama 2 jam mempunyai konduktivitas listrik tertinggi yaitu 2,4 × 10-6 S/cm.

Kata kunci: abudasar, hidrotermal, konduktivitas, nosean, sodalit, zeolit

Downloads

Published

2017-07-05

How to Cite

Nurhabibah, N., & Muttaqin, A. (2017). Pengaruh Variasi Waktu Peleburan Terhadap Konduktivitas Listrik Zeolit dari Abu Dasar Batubara yang Disintesis dengan Metode Peleburan Alkali Hidrotermal. Jurnal Fisika Unand, 6(3), 240–246. https://doi.org/10.25077/jfu.6.3.240-246.2017

Issue

Vol. 6 No. 3 (2017)

Section

Articles

License

Copyright (c) 2017 Nurhabibah Nurhabibah, Afdhal Muttaqin

Creative Commons License

This work is licensed under a Creative Commons Attribution-NonCommercial 4.0 International License.

Please find the rights and licenses in JFU (Jurnal Fisika Unand).

1. License

The non-commercial use of the article will be governed by the Creative Commons Attribution license as currently displayed on Creative Commons Attribution-NonCommercial 4.0 International License.

2. Authors Warranties

The author warrants that the article is original, written by stated author(s), has not been published before, contains no unlawful statements, does not infringe the rights of others, is subject to copyright that is vested exclusively in the author and free of any third party rights, and that any necessary written permissions to quote from other sources have been obtained by the author(s).

3. User Rights

JFU's spirit is to disseminate articles published are as free as possible. Under the Creative Commons license, JFU permits users to copy, distribute, display, and perform the work for non-commercial purposes only. Users will also need to attribute authors and JFU on distributing works in the journal.

4. Rights of Authors

Authors retain the following rights:

  • Copyright, and other proprietary rights relating to the article, such as patent rights,
  • The right to use the substance of the article in future own works, including lectures and books,
  • The right to reproduce the article for own purposes, provided the copies are not offered for sale,
  • The right to self-archive the article.

5. Co-Authorship

If the article was jointly prepared by other authors, the signatory of this form warrants that he/she has been authorized by all co-authors to sign this agreement on their behalf, and agrees to inform his/her co-authors of the terms of this agreement.

6. Termination

This agreement can be terminated by the author or JFU upon two months notice where the other party has materially breached this agreement and failed to remedy such breach within a month of being given the terminating partys notice requesting such breach to be remedied. No breach or violation of this agreement will cause this agreement or any license granted in it to terminate automatically or affect the definition of JFU.

7. Royalties

This agreement entitles the author to no royalties or other fees. To such extent as legally permissible, the author waives his or her right to collect royalties relative to the article in respect of any use of the article by JFU or its sublicensee.

8. Miscellaneous

JFU will publish the article (or have it published) in the journal if the articles editorial process is successfully completed and JFU or its sublicensee has become obligated to have the article published. JFU may conform the article to a style of punctuation, spelling, capitalization, referencing and usage that it deems appropriate. The author acknowledges that the article may be published so that it will be publicly accessible and such access will be free of charge for the readers.