Karakterisasi Sensor TiO2 Didoping ZnO untuk Mendeteksi Gas Oksigen
DOI:
https://doi.org/10.25077/jfu.5.2.122-130.2016Abstract
Telah dilakukan karakterisasi sensor gas oksigen berupa pelet dengan bahan utama TiO2 didoping dengan ZnO. Pelet sensor gas oksigen dibuat dengan variasi doping ZnO (0% mol, 2% mol,4% mol, 6%mol, 8% mol, dan 10% mol) terhadap bahan utama TiO2. Proses pembuatan sensor gas oksigen diawali dengan pencampuran bahan TiO2 didoping ZnO, kalsinasi pada temperatur 800 ºC selama 4 jam, penggerusan, kompaksi, dan sintering pada temperatur 900 ºC selama 4 jam. Sensor gas oksigen diuji pada temperatur ruang (30 ºC) dengan melihat karakteristik I-V, nilai sensitivitas, nilai konduktivitas, waktu respon, dan karakterisasi XRD. Berdasarkan pengukuran krakteristik I-V bahwa sampel dengan penambahan bahan ZnO sebanyak 8% mol memiliki sensitivitas tertinggi dibanding sampel lainnya yaitu 2,46 pada tegangan 3 volt dan sampel yang memiliki konduktivitas tertinggi terdapat pada sampel dengan penambahan ZnO terbanyak yaitu 10% mol dengan nilai konduktivitas di lingkungan udara sebesar 7,33 x 10-3 Ω-1m-1 dan nilai konduktivitas di lingkungan oksigen sebesar 11,79 x 10-3 Ω-1m-1. Waktu respon sampel 92% mol TiO2 + 8% ZnO pada tegangan 3 volt adalah 55 s. Hasil XRD menunjukkan ukuran kristal 92% mol TiO2 + 8% mol ZnO lebih besar dibandingkan dengan bahan TiO2 murni. Pada doping TiO2 + 8% ZnO telah terbentuk senyawa baru berupa Zn2TiO4.
Kata kunci : karakterisasi I-V, konduktivitas, sensor gas oksigen,sensitivitas, TiO2(ZnO),waktu respon.
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Copyright (c) 2016 Wahyuni Putri, Elvaswer Elvaswer
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