Ekstraksi dan Karakterisasi Hidroksiapatit (HAp) dari Tulang Ikan Tenggiri (Scomberomorus commersoni) dengan Metode Heat Treatment

Authors

  • Rodearni Ananda Putri Purba Universitas Jambi
  • Tika Restianingsih Universitas Jambi
  • Rista Mutia Anggraini Universitas Jambi
  • Yoza Fendriani Universitas Jambi
  • Frastica Deswardani Universitas Jambi

DOI:

https://doi.org/10.25077/jfu.13.2.247-253.2024

Keywords:

Hidroksiapatit, Heat Treatment, XRD, FTIR

Abstract

Telah dilakukan ekstraksi hidroksiapatit (HAp) dari tulang ikan tenggiri (Scomberomorus commersoni) menggunakan metode heat treatment. Penelitian bertujuan melihat pengaruh suhu yang  diberikan kepada sampel terhadap ukuran kristal dan derajat kristalinitas. Heat treatment dilakukan pada suhu 400OC, 600OC dan 800OC masing-masing selama 3 jam terhadap sampel yang telah di preparasi. Hasil analisis XRD menunjukkan adanya puncak  yang terbentuk pada sudut 2θ 25,950; 31,880; 39,620; 44,410; 46,700; 49,400 untuk suhu 400OC, 31,780; 32,800; 34,610 pada suhu 600OC dan 31,760; 32,210; 32,940; 34,070 pada suhu 800OC yang disesuaikan dengan referensi JCPDS 090432. Pada suhu 400OC, 600OC dan 800OC diperoleh ukuran kristal berturut-turut 12,05 nm, 14,18 nm dan  42,55 nm dan  derajat kristalinitas bernilai 41,91%, 76,38% dan 87,29%. Spektrum FTIR menunjukkan bahwa, semakin tinggi suhu maka lembah yang terbentuk semakin tajam dan adanya gugus fungsi OH-, dan  yang merupakan karakteristik dari gugus fungsi HAp, selain itu muncul pula gugus H2O. Karakterisasi SEM menunjukkan morfologi berbentuk bulk.

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Published

2024-03-05

How to Cite

Purba, R. A. P., Restianingsih, T., Anggraini, R. M., Fendriani, Y., & Deswardani, F. (2024). Ekstraksi dan Karakterisasi Hidroksiapatit (HAp) dari Tulang Ikan Tenggiri (Scomberomorus commersoni) dengan Metode Heat Treatment. Jurnal Fisika Unand, 13(2), 247–253. https://doi.org/10.25077/jfu.13.2.247-253.2024

Issue

Vol. 13 No. 2 (2024)

Section

Articles

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